JPH0150690B2 - - Google Patents
Info
- Publication number
- JPH0150690B2 JPH0150690B2 JP18879683A JP18879683A JPH0150690B2 JP H0150690 B2 JPH0150690 B2 JP H0150690B2 JP 18879683 A JP18879683 A JP 18879683A JP 18879683 A JP18879683 A JP 18879683A JP H0150690 B2 JPH0150690 B2 JP H0150690B2
- Authority
- JP
- Japan
- Prior art keywords
- acid ester
- acid
- fluoro
- fluoroacrylic
- dehydrating agent
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 claims description 16
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims description 14
- -1 α-fluoroacrylic acid ester Chemical class 0.000 claims description 14
- 229910000147 aluminium phosphate Inorganic materials 0.000 claims description 8
- 239000012024 dehydrating agents Substances 0.000 claims description 6
- DLYUQMMRRRQYAE-UHFFFAOYSA-N tetraphosphorus decaoxide Chemical compound O1P(O2)(=O)OP3(=O)OP1(=O)OP2(=O)O3 DLYUQMMRRRQYAE-UHFFFAOYSA-N 0.000 claims description 6
- 238000004519 manufacturing process Methods 0.000 claims description 5
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 9
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 6
- 238000006243 chemical reaction Methods 0.000 description 6
- QIGBRXMKCJKVMJ-UHFFFAOYSA-N Hydroquinone Chemical compound OC1=CC=C(O)C=C1 QIGBRXMKCJKVMJ-UHFFFAOYSA-N 0.000 description 4
- YWEUIGNSBFLMFL-UHFFFAOYSA-N diphosphonate Chemical compound O=P(=O)OP(=O)=O YWEUIGNSBFLMFL-UHFFFAOYSA-N 0.000 description 4
- WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 description 3
- 238000006116 polymerization reaction Methods 0.000 description 3
- 239000002994 raw material Substances 0.000 description 3
- YCIMNLLNPGFGHC-UHFFFAOYSA-N catechol Chemical compound OC1=CC=CC=C1O YCIMNLLNPGFGHC-UHFFFAOYSA-N 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 230000018044 dehydration Effects 0.000 description 2
- 238000006297 dehydration reaction Methods 0.000 description 2
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 229920000642 polymer Polymers 0.000 description 2
- 239000002904 solvent Substances 0.000 description 2
- MIZLGWKEZAPEFJ-UHFFFAOYSA-N 1,1,2-trifluoroethene Chemical group FC=C(F)F MIZLGWKEZAPEFJ-UHFFFAOYSA-N 0.000 description 1
- KEQGZUUPPQEDPF-UHFFFAOYSA-N 1,3-dichloro-5,5-dimethylimidazolidine-2,4-dione Chemical compound CC1(C)N(Cl)C(=O)N(Cl)C1=O KEQGZUUPPQEDPF-UHFFFAOYSA-N 0.000 description 1
- SVYXLQRWNWOHSJ-UHFFFAOYSA-N 2-fluoro-3-hydroxypropanoic acid Chemical compound OCC(F)C(O)=O SVYXLQRWNWOHSJ-UHFFFAOYSA-N 0.000 description 1
- TYCFGHUTYSLISP-UHFFFAOYSA-N 2-fluoroprop-2-enoic acid Chemical class OC(=O)C(F)=C TYCFGHUTYSLISP-UHFFFAOYSA-N 0.000 description 1
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 1
- JVTAAEKCZFNVCJ-UHFFFAOYSA-M Lactate Chemical compound CC(O)C([O-])=O JVTAAEKCZFNVCJ-UHFFFAOYSA-M 0.000 description 1
- 150000001298 alcohols Chemical class 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- XTHPWXDJESJLNJ-UHFFFAOYSA-N chlorosulfonic acid Substances OS(Cl)(=O)=O XTHPWXDJESJLNJ-UHFFFAOYSA-N 0.000 description 1
- 238000009833 condensation Methods 0.000 description 1
- 230000005494 condensation Effects 0.000 description 1
- 238000005336 cracking Methods 0.000 description 1
- ZYMKZMDQUPCXRP-UHFFFAOYSA-N fluoro prop-2-enoate Chemical compound FOC(=O)C=C ZYMKZMDQUPCXRP-UHFFFAOYSA-N 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 239000003112 inhibitor Substances 0.000 description 1
- JVTAAEKCZFNVCJ-UHFFFAOYSA-N lactic acid Chemical class CC(O)C(O)=O JVTAAEKCZFNVCJ-UHFFFAOYSA-N 0.000 description 1
- 125000005397 methacrylic acid ester group Chemical group 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- ZTZJVAOTIOAZGZ-UHFFFAOYSA-N methyl 2-fluoroacrylate Chemical compound COC(=O)C(F)=C ZTZJVAOTIOAZGZ-UHFFFAOYSA-N 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 239000013307 optical fiber Substances 0.000 description 1
- 239000003973 paint Substances 0.000 description 1
- 239000011541 reaction mixture Substances 0.000 description 1
- 238000010992 reflux Methods 0.000 description 1
- 239000004065 semiconductor Substances 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000005979 thermal decomposition reaction Methods 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP18879683A JPS6078941A (ja) | 1983-10-07 | 1983-10-07 | α−フルオロアクリル酸エステルの製造法 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP18879683A JPS6078941A (ja) | 1983-10-07 | 1983-10-07 | α−フルオロアクリル酸エステルの製造法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS6078941A JPS6078941A (ja) | 1985-05-04 |
| JPH0150690B2 true JPH0150690B2 (en]) | 1989-10-31 |
Family
ID=16229947
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP18879683A Granted JPS6078941A (ja) | 1983-10-07 | 1983-10-07 | α−フルオロアクリル酸エステルの製造法 |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS6078941A (en]) |
Families Citing this family (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20050221457A1 (en) * | 2002-03-25 | 2005-10-06 | Paraskevas Tsobanakis | Methods of manufacturing derivatives of beta-hydroxycarboxylic acids |
| JP5277837B2 (ja) * | 2008-09-26 | 2013-08-28 | セントラル硝子株式会社 | α−トリフルオロメチル−α，β−不飽和エステル類の製造方法 |
| JP5240078B2 (ja) * | 2009-06-09 | 2013-07-17 | セントラル硝子株式会社 | ２−フルオロアクリル酸エステルの製造方法 |
| DE102009030681A1 (de) * | 2009-06-26 | 2010-12-30 | Saltigo Gmbh | Herstellung von substituierten 2-Fluoracrylsäurederivaten |
| JP6237223B2 (ja) * | 2012-12-28 | 2017-11-29 | ダイキン工業株式会社 | α−フルオロアクリル酸エステルの製造方法 |
| WO2015058116A1 (en) | 2013-10-17 | 2015-04-23 | Cargill, Incorporated | Methods for producing alkyl hydroxyalkanoates |
| US10239819B2 (en) | 2014-10-17 | 2019-03-26 | Cargill, Incorporated | Methods for producing an ester of an alpha, beta-unsaturated carboxylic acid |
| EP4053099A3 (en) * | 2015-04-09 | 2022-11-30 | Daikin Industries, Ltd. | Acrylic acid derivative-containing composition, and method for stabilizing acrylic acid derivative |
-
1983
- 1983-10-07 JP JP18879683A patent/JPS6078941A/ja active Granted
Also Published As
| Publication number | Publication date |
|---|---|
| JPS6078941A (ja) | 1985-05-04 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| JPH04283529A (ja) | ４−ヒドロキシスチレンの製造方法 | |
| JPH0321619A (ja) | トリオキサン及びトリメチロールプロパンホルマール誘導体の新規なポリアセタールコポリマー | |
| JPH0150690B2 (en]) | ||
| JPH05507936A (ja) | 環式サルフェートの製造法 | |
| US4228305A (en) | Process for preparing acetic acid derivatives | |
| JPS5883028A (ja) | ポリテトラメチレングリコ−ルの製造方法 | |
| WO2005040246A1 (ja) | アシロキシ酢酸重合体およびその製造方法 | |
| JPH02193944A (ja) | （メタ）アクリル酸エステルの製造方法 | |
| JPS5826838A (ja) | ３−ブロモ−４−フルオロベンズアルデヒドの製造方法 | |
| Wang et al. | Effect of para substitution on the rate of alkaline hydrolysis of ethyl 5-phenyl-2, 4-pentadienoates | |
| JP2867644B2 (ja) | 反応性樹脂の製造方法 | |
| JP7676261B2 (ja) | ２－メチレン－１，３－プロパンジオールジアセテートの製造方法及び変性エチレン－ビニルエステル共重合体の製造方法 | |
| JP2007112788A (ja) | オキセタン化合物 | |
| JPS6078943A (ja) | α−フルオロアクリル酸エステルの製法 | |
| US2161552A (en) | Esters of phthalic acid | |
| JPS58152831A (ja) | フルオロジケトン類の製造方法 | |
| JPS5839680A (ja) | ケタ−ル化されたグリセロ−ルアリルエ−テルの合成法 | |
| CN112592270A (zh) | 一种2-卤代-2,2-二氟乙酸烯酯的制备方法 | |
| KR100650143B1 (ko) | 알콕시폴리알킬렌글리콜(메타)아크릴레이트의 제조방법 | |
| CN101270046A (zh) | 熔融酯化法制备丙烯酸十八酯的工艺 | |
| JPS5993064A (ja) | アセトニルイソシアヌレ−トの製造法 | |
| JPS5936976B2 (ja) | ビス（４−ヒドロキシフエニル）スルホン誘導体の製造方法 | |
| JPH1072379A (ja) | イソブチレンおよびメタクリル酸エステルの製造方法 | |
| JPS6038386B2 (ja) | グリシジルオレイルエ−テルの製造法 | |
| JPS58206546A (ja) | アルキルアクリルアミドグリコレ−ト及びそのアルキルエ−テルの製造方法 |